PH626, 986---Electron Microscopy (Spring Semester)
Goal
This is a hands-on training intended to provide the necessary individual practical
training in the methods of transmission electron microscopy, instrumental
techniques and interpretative application of contrast and diffraction principles,
to enable students to apply this method of structural characterization to
problems connected with their research projects. Small group laboratory session
are given to make the students confident with operation of the instrument.
A series of exercises are carried out by each student to afford practice in
the various capabilities of the TEM method. The students should be able to
operate the microscope independently after this training course.
Contents
* Load and unload sample
* Get the beam
* Alignment
* Obtaining an electron diffraction pattern (EDP)
* Index an EDP
* Tilting an EDP into zone axis
* Phase identification by EDPs
* Obtaining bright-field and dark-field images
* Defects study
* Take a photo
* Dark room
* Sample preparation
* TEM software
Grade
* Attendance of class
* Assignment
* Final Project